Catalytic Synthesis of n-Amyl Benzoate with TiSiW_(12)O_(40)/TiO_2
Yong Liang
Abstract
Yong Liang
Abstract
The synthesis of n-amyl benzoate was studied with pent a nol and phenylformic acid as reactants,and reaction conditions were selected. It showed that TiSiW 12O 40/TiO 2 was an excellent catalyst for the syn thesis of n-amyl benzoate, and the optimum reaction conditions were that the mol ar ratio of pentyl to acid was 4:1, the mass ratio of the catalyst used in the r eactants was 1.5%, and the reaction time was 2.5 h. Under these conditions, the yield of n-amyl benzoate reached 96.7%.
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The synthesis of n-amyl benzoate was studied with pent a nol and phenylformic acid as reactants,and reaction conditions were selected. It showed that TiSiW 12O 40/TiO 2 was an excellent catalyst for the syn thesis of n-amyl benzoate, and the optimum reaction conditions were that the mol ar ratio of pentyl to acid was 4:1, the mass ratio of the catalyst used in the r eactants was 1.5%, and the reaction time was 2.5 h. Under these conditions, the yield of n-amyl benzoate reached 96.7%.
Key concepts: Catalysis, Yield (engineering), Chemistry, Reaction conditions, Benzyl benzoate, Organic chemistry, Nuclear chemistry, Medicinal chemistry