2000•Journal of Qingdao UniversityRequires access

SYNTHESIS OF N-AMYL BUTYRATE BY USING TiSiW_(12)O_(40)/TiO_2 AS CATALYST

Yang Shui-jin

Abstract

The synthesis of n-amyl butyrate using TiSiW12O40/TiO2 as catalyst has been studied. The optimum conditions are: molar ratio of n-amyl to butyl acid is 1.3:1, the quantity of catalyst is equal to 1.5% feed stock, the reaction temperature is 125-135℃, and the reaction time is 1.0h. TiSiW12O40/TiO2 is an excellent catalyst for synthetizing n-amyl butyrate and its yield can reach over 98.9%.

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Key concepts: Catalysis, Molar ratio, Butyrate, Yield (engineering), Chemistry, Nuclear chemistry, Organic chemistry, Materials science