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Catalytic synthesis of n-amyl benzoate with TiSiW_(12)O_(40)/TiO_2

Bin Hu

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Abstract

The synthesis of n amyl benzoate were studied with amyl alcohol and phenylformic acid as reactants,and reaction conditions were selected.It showed that TiSiW 12 O 40 /TiO 2 was an excellent catalyst for the synthesis of n amyl benzoate,and the optimun reaction conditions was that the molar ratio of pentyl to acid was 4∶1,the mass ratio of the catalyst used to the reactants was 1.5%,and the reaction time was 2.5 h. Under above conditions,the yield of n amyl benzoate reached 96.7%.

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What this paper is about

The synthesis of n amyl benzoate were studied with amyl alcohol and phenylformic acid as reactants,and reaction conditions were selected.It showed that TiSiW 12 O 40 /TiO 2 was an excellent catalyst for the synthesis of n amyl benzoate,and the optimun reaction conditions was that the molar ratio of pentyl to acid was 4∶1,the mass ratio of the catalyst used to the reactants was 1.5%,and the reaction time was 2.5 h. Under above conditions,the yield of n amyl benzoate reached 96.7%.

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Available abstract

The synthesis of n amyl benzoate were studied with amyl alcohol and phenylformic acid as reactants,and reaction conditions were selected.It showed that TiSiW 12 O 40 /TiO 2 was an excellent catalyst for the synthesis of n amyl benzoate,and the optimun reaction conditions was that the molar ratio of pentyl to acid was 4∶1,the mass ratio of the catalyst used to the reactants was 1.5%,and the reaction time was 2.5 h. Under above conditions,the yield of n amyl benzoate reached 96.7%.

Key concepts: Catalysis, Molar ratio, Chemistry, Yield (engineering), Alcohol, Benzyl benzoate, Organic chemistry, Reaction conditions

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