2001•Unpublished venueRequires access

Synthesis of propyl chloroacetate by using TiSiW_(12)O_(40)/TiO_2 as catalyst

Liang Yong

Abstract

The synthesis propyl chloroacetate of using TiSiW 12 O 40 /TiO 2 as catalyst has been studied.The factors influencing the synthesis were discussed and the best conditions were found out.The optimum conditions are:molar ratio of propanol to chloroacetic acid is 1.4∶1,the quantity of catalyst is equal to 2.0% feed stock,the reaction temperature is 95-110℃,and the reaction time is 2.0h.TiSiW 12 O 40 /TiO 2 is an excellent catalyst for synthetizing propyl chloroacetate and its yield can reach over 77.14%.

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Key concepts: Chloroacetic acid, Catalysis, Molar ratio, Ethyl chloroacetate, Chemistry, Yield (engineering), Reaction conditions, Nuclear chemistry