Catalytic synthesis of propyl benzoate with TiSiW_(12)O_(40)/TiO_2
Liang Yong-guang
Abstract
Liang Yong-guang
Abstract
The catalytic activities of TiSiW 12O 40/TiO 2 in synthesizing propyl benzoate are reported. It has been demonstrated that TiSiW 12O 40/TiO 2 is an excellent catalyst.Various factors concerned in this reaction have been investigated.The optimum conditions have been found,that is,the molar ratio of alcohol to acid is 4∶1,the mass ratio of the catalyst used to the reactants was 1.5%,the reaction time 2.5 h.Under this conditions,the yield of propyl benzoate is 70.5%.
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The catalytic activities of TiSiW 12O 40/TiO 2 in synthesizing propyl benzoate are reported. It has been demonstrated that TiSiW 12O 40/TiO 2 is an excellent catalyst.Various factors concerned in this reaction have been investigated.The optimum conditions have been found,that is,the molar ratio of alcohol to acid is 4∶1,the mass ratio of the catalyst used to the reactants was 1.5%,the reaction time 2.5 h.Under this conditions,the yield of propyl benzoate is 70.5%.
Key concepts: Catalysis, Molar ratio, Yield (engineering), Chemistry, Alcohol, Reaction conditions, Nuclear chemistry, Organic chemistry