2001•Journal Fo Molecular ScienceRequires access
Hydrothermal synthesis and characterization of a novel compound [(2,2-bipy)_2(VO_2)_2(HPO_4)]·H_2O
Lu’an Guo
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Abstract
A novel compound, [(2,2-bipy) 2(VO 2) 2(HPO 4)]·H 2O was first prepared by hydrothermal synthesis and characterized by elemental analysis, IR, and single crystal X-ray diffraction. Crystal data:monoclinic, space group P2 1/n,a =0.921 6(2) nm, b = 1.617 7(3)nm , c =1.532 1(3)nm, V =2.254 3(8)nm 3, β =99.28(2)°, Z =4, D c=1 745 kg/m 3, F (000) = 1 200 , R =0.036 5, wR 2=0.082 7.