2002•Journal Fo Molecular ScienceRequires access
Hydrothermal synthesis and crystal structure of a novel super molecular compound (H_3NCH_2CH_2NH_3)_2[(HPO_4)_2Mo_5O_(15)]
Lu’an Guo
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Abstract
A novel super molecular compound,(H 3NCH 2CH 2NH 3) 2[(HPO 4) 2Mo 5O 15 ],was hydrothermally synthesized and structurally characterized by single crystal X-ray diffraction.The compound crystallizes in monoclinic space,group C2/c with a= 1 766 6(4) nm, b =1 003 4(2)nm, c =1 376 7(3)nm, α=90°,β=96 90(3)°,γ=90°,V=2 422 7(8) nm 3, Z=4,R=0 0431,wR 2=0 128 7.