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2013•Journal of Jilin Institute of Chemical TechnologyRequires access

Synthesis,Structure and Electrochemical Property of a New Compound [Cu(bipy)(SiMo_(12)O_(40))_(0.5)](H_2bipy)_0.5·H_2O

DU Hai-fen

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Abstract

[Cu(bipy)(SiMo12O40)0.5](H2bipy)0.5·H2O(1) has been synthesized under hydrothermal conditions and was characterized by elemental analysiss such as IR and single-crystal X-ray diffraction.X-ray analyses reveals that compound 1 crystallizes in the triclinic system,space group p-1,a=1.084 85(6) nm,b=1.179 30(7) nm,c=1.328 96(8) nm,α=105.328(5) °,β=102.773(5) °,γ=114.872(6) °,V=1.376 21(14) nm3,Z=2,R 1=0.047 9,ωR 2=0.116 0.Compound 1 represents a one dimensional doublechains structure.Furthermore,the electrochemical property of compound 1 has been studied.

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What this paper is about

[Cu(bipy)(SiMo12O40)0.5](H2bipy)0.5·H2O(1) has been synthesized under hydrothermal conditions and was characterized by elemental analysiss such as IR and single-crystal X-ray diffraction.X-ray analyses reveals that compound 1 crystallizes in the triclinic system,space group p-1,a=1.084 85(6) nm,b=1.179 30(7) nm,c=1.328 96(8) nm,α=105.328(5) °,β=102.773(5) °,γ=114.872(6) °,V=1.376 21(14) nm3,Z=2,R 1=0.047 9,ωR 2=0.116 0.Compound 1 represents a one dimensional doublechains structure.Furthermore,the electrochemical property of compound 1 has been studied.

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Available abstract

[Cu(bipy)(SiMo12O40)0.5](H2bipy)0.5·H2O(1) has been synthesized under hydrothermal conditions and was characterized by elemental analysiss such as IR and single-crystal X-ray diffraction.X-ray analyses reveals that compound 1 crystallizes in the triclinic system,space group p-1,a=1.084 85(6) nm,b=1.179 30(7) nm,c=1.328 96(8) nm,α=105.328(5) °,β=102.773(5) °,γ=114.872(6) °,V=1.376 21(14) nm3,Z=2,R 1=0.047 9,ωR 2=0.116 0.Compound 1 represents a one dimensional doublechains structure.Furthermore,the electrochemical property of compound 1 has been studied.

Key concepts: Triclinic crystal system, Electrochemistry, Crystal structure, Hydrothermal synthesis, Crystallography, Hydrothermal circulation, Chemistry, Diffraction

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Synthesis,Structure and Electrochemical Property of a New Compound [Cu(bipy)(SiMo_(12)O_(40))_(0.5)](H_2bipy)_0.5·H_2O — Research Paper | ScholarLens