2011•Journal of Northeast Normal UniversityRequires access

Hydrothermal synthesis,characterization of a super molecular compound [(4,4′-bipy)_4H_5][BW_(12)O_(40)]·2H_2O

Jia Rui-xia

Abstract

A super molecular complex [(4,4′-bipy)4H5][BW12O40]·2H2O was synthesized by IR,elemental analyses and single-crystal X-ray diffraction.The crystal data for this compound are the following:monoclinic,space group C2/C,a=2.179 5(5) nm,b=1.393 9(5) nm,c=2.128 9(5) nm,α=90°,β=104.166(5)°,γ=90°,V=6.271(3) nm3,Z=4,R1=0.072 5,wR2=0.294 3.

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Key concepts: Monoclinic crystal system, Crystallography, Hydrothermal synthesis, Hydrothermal circulation, Chemistry, Single crystal, Diffraction, Crystal structure