2010Journal of Liaocheng UniversityRequires access

Synthesis and Crystal Structure of the Schiff Base Derived from 2-Hydroxy-1-naphthaldehyde and m-Aminobenzoic Acid

Li Guo

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Abstract

The Schiff base derived from 2-Hydroxy-1-naphthaldehyde and m-aminobenzoicacid was synthesized.The title compound was characterized by IR,UV spectra,elemental analysis.The crystal structure of Schiff base have been determined by single crystal X-ray diffraction analysis.The crystal belongs to monoclinic,space group P2(1)/c with a=1.165 4(4) nm,b=0.746 5(2) nm,c=1.626 4(5) nm,α=90°,β=106.665°,γ=90°,Z=4,V=1.355 5(8) nm3,Dc=1.427 0 g/cm3,μ=0.098 0 mm-1,F(000)=608,R=0.046 7 and wR=0.108 0.

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The Schiff base derived from 2-Hydroxy-1-naphthaldehyde and m-aminobenzoicacid was synthesized.The title compound was characterized by IR,UV spectra,elemental analysis.The crystal structure of Schiff base have been determined by single crystal X-ray diffraction analysis.The crystal belongs to monoclinic,space group P2(1)/c with a=1.165 4(4) nm,b=0.746 5(2) nm,c=1.626 4(5) nm,α=90°,β=106.665°,γ=90°,Z=4,V=1.355 5(8) nm3,Dc=1.427 0 g/cm3,μ=0.098 0 mm-1,F(000)=608,R=0.046 7 and wR=0.108 0.

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Available abstract

The Schiff base derived from 2-Hydroxy-1-naphthaldehyde and m-aminobenzoicacid was synthesized.The title compound was characterized by IR,UV spectra,elemental analysis.The crystal structure of Schiff base have been determined by single crystal X-ray diffraction analysis.The crystal belongs to monoclinic,space group P2(1)/c with a=1.165 4(4) nm,b=0.746 5(2) nm,c=1.626 4(5) nm,α=90°,β=106.665°,γ=90°,Z=4,V=1.355 5(8) nm3,Dc=1.427 0 g/cm3,μ=0.098 0 mm-1,F(000)=608,R=0.046 7 and wR=0.108 0.

Key concepts: Monoclinic crystal system, Schiff base, Crystal structure, Crystallography, Chemistry, Crystal (programming language), Single crystal, Base (topology)

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