Studies on the chemical constituents of Ainsliaea macrocephala
Yunheng Shen
Abstract
Yunheng Shen
Abstract
Objective To study the chemical constituents of Ainsliaea macrocephala(Franch).Methods The isolation and purification were carried out by extraction,silica gel and Sephadex LH-20 column chromatography.The compounds were identified on the basis of spectral analysis,including IR,1H-NMR,13C-NMR and MS.Results Six compounds were obtained from petrol ether fraction of ethnol extract of Ainsliaea macrocephala and their structures were determined as simiarenol(1),stigmasterol(2),Bis(2-ethylhexy1) phthalate(3),octadecanoic acid(4),2-hydroxy-linolenic acid(5),glycerol-tri-9-octadecenoate(6).Conclusion Compounds(1)~(6) were isolated from this plant for the first time.
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Objective To study the chemical constituents of Ainsliaea macrocephala(Franch).Methods The isolation and purification were carried out by extraction,silica gel and Sephadex LH-20 column chromatography.The compounds were identified on the basis of spectral analysis,including IR,1H-NMR,13C-NMR and MS.Results Six compounds were obtained from petrol ether fraction of ethnol extract of Ainsliaea macrocephala and their structures were determined as simiarenol(1),stigmasterol(2),Bis(2-ethylhexy1) phthalate(3),octadecanoic acid(4),2-hydroxy-linolenic acid(5),glycerol-tri-9-octadecenoate(6).Conclusion Compounds(1)~(6) were isolated from this plant for the first time.
Key concepts: Chemistry, Sephadex, Column chromatography, Stigmasterol, Chemical constituents, Chromatography, Silica gel, Ether