2004Shaanxi Chemical IndustryRequires access

Catalytic synthesis of methyl 1-naphthyl acetate with aminosulfonic acid

XU Dong-fang

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Abstract

The optimum conditions have been studied on which the 1-naphthaleneacetic acid and methanol are esterified into methyl 1-naphthyl acetate in the presence of the aminosulfonic acid, and the reuseability of the catalyst. The yield of the ester could reach 97.5% when the mole ratio of 1-naphthaleneacetic acid, methanol and aminosulfonic acid was 1∶10∶1.05, and the mixture was refluxing for 5 h.

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What this paper is about

The optimum conditions have been studied on which the 1-naphthaleneacetic acid and methanol are esterified into methyl 1-naphthyl acetate in the presence of the aminosulfonic acid, and the reuseability of the catalyst. The yield of the ester could reach 97.5% when the mole ratio of 1-naphthaleneacetic acid, methanol and aminosulfonic acid was 1∶10∶1.05, and the mixture was refluxing for 5 h.

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Available abstract

The optimum conditions have been studied on which the 1-naphthaleneacetic acid and methanol are esterified into methyl 1-naphthyl acetate in the presence of the aminosulfonic acid, and the reuseability of the catalyst. The yield of the ester could reach 97.5% when the mole ratio of 1-naphthaleneacetic acid, methanol and aminosulfonic acid was 1∶10∶1.05, and the mixture was refluxing for 5 h.

Key concepts: Catalysis, Methanol, Chemistry, Yield (engineering), Methyl acetate, Organic chemistry, Nuclear chemistry, Materials science

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