2006Journal of Henan University of TechnologyRequires access

SYNTHESIS OF β-NAPHTHYL ACETATE CATALYZED BY AMINOSULFONIC ACID

Qiao Wang

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Abstract

β-Naphthyl aceate was synthesized with acetic anhydride and naphthol using aminosulfonic acid as catalyst.The yield of β-naphthyl acetate was 97.8% under the optimum conditions: β-naphthlol 7.2 g(0.05 mol),acetic anhydride 6 mL(0.06 mol),aminosulfonic acid 1.0 g,reaction time 30 min,80 ℃.The reaction time was short and the catalyst could be recovered and reused for more than 4 times.

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β-Naphthyl aceate was synthesized with acetic anhydride and naphthol using aminosulfonic acid as catalyst.The yield of β-naphthyl acetate was 97.8% under the optimum conditions: β-naphthlol 7.2 g(0.05 mol),acetic anhydride 6 mL(0.06 mol),aminosulfonic acid 1.0 g,reaction time 30 min,80 ℃.The reaction time was short and the catalyst could be recovered and reused for more than 4 times.

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Available abstract

β-Naphthyl aceate was synthesized with acetic anhydride and naphthol using aminosulfonic acid as catalyst.The yield of β-naphthyl acetate was 97.8% under the optimum conditions: β-naphthlol 7.2 g(0.05 mol),acetic anhydride 6 mL(0.06 mol),aminosulfonic acid 1.0 g,reaction time 30 min,80 ℃.The reaction time was short and the catalyst could be recovered and reused for more than 4 times.

Key concepts: Acetic anhydride, Catalysis, Acetic acid, Yield (engineering), Chemistry, Nuclear chemistry, Organic chemistry, Materials science

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