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Synthesis of n-Butyl Benzoate Catalyzed by Ti(SO_4)_2/SiO_2

Sheng Shu-ling

Abstract

n-Butyl benzoate was synthesized from benzoic acid and n-butyl alcohol using Ti (SO4)2/SiO2 as catalyst.The factors influencing the synthesis were discussed and best conditions were found out. The optimum conditions are:molar ratio of alcohol to acid was 3:1,the amount of catalyst was 2.5 g/0.05 mol benzoic acid, the reaction time was 2 h.Ti(SO4)2/SiO2 was a good catalyst for synthesizing n-butyl benzoate and its yield can reach up to 96.1%.

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Key concepts: Benzoic acid, Catalysis, Molar ratio, Yield (engineering), Alcohol, Chemistry, Nuclear chemistry, Organic chemistry