2012Japanese Journal of Applied PhysicsOpen access

Synthesis of TiO2Nanowires via Hydrothermal Method

Asiah Mohd Nor, M.F. Achoi, Mohamad Hafiz Mamat, Musa Mohamed Zabidi, Saifollah Abdullah, Mohamad Rusop Mahmood

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Abstract

Titanium dioxide (TiO2) nanowires have been successfully synthesized by a simple, rapid, inexpensive, and novel approach based on a hydrothermal method. The use of hydrothermal treatment on TiO2nanopowder as a precursor with highly concentrated sodium hydroxide for 6 h produced a novel nanostructure of TiO2nanowires. The field-emission scanning electron microscopy (FESEM) image shows that the synthesized TiO2nanowires are very abundant in quantity with diameters ranging from 8.0–14 nm and are extra long. X-ray diffraction (XRD) result indicates that the synthesized TiO2nanowires are mainly composed of anatase phase with a minor of rutile phase. These properties of nanowires promise a broad range of applications in electronic devices.

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Titanium dioxide (TiO2) nanowires have been successfully synthesized by a simple, rapid, inexpensive, and novel approach based on a hydrothermal method. The use of hydrothermal treatment on TiO2nanopowder as a precursor with highly concentrated sodium hydroxide for 6 h produced a novel nanostructure of TiO2nanowires. The field-emission scanning electron microscopy (FESEM) image shows that the synthesized TiO2nanowires are very abundant in quantity with diameters ranging from 8.0–14 nm and are extra long. X-ray diffraction (XRD) result indicates that the synthesized TiO2nanowires are mainly composed of anatase phase with a minor of rutile phase. These properties of nanowires promise a broad range of applications in electronic devices.

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Available abstract

Titanium dioxide (TiO2) nanowires have been successfully synthesized by a simple, rapid, inexpensive, and novel approach based on a hydrothermal method. The use of hydrothermal treatment on TiO2nanopowder as a precursor with highly concentrated sodium hydroxide for 6 h produced a novel nanostructure of TiO2nanowires. The field-emission scanning electron microscopy (FESEM) image shows that the synthesized TiO2nanowires are very abundant in quantity with diameters ranging from 8.0–14 nm and are extra long. X-ray diffraction (XRD) result indicates that the synthesized TiO2nanowires are mainly composed of anatase phase with a minor of rutile phase. These properties of nanowires promise a broad range of applications in electronic devices.

Key concepts: Nanowire, Anatase, Hydrothermal circulation, Rutile, Materials science, Titanium dioxide, Scanning electron microscope, Nanotechnology

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