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Synthesis and crystal structure of 3D network Zn(II) complex

Yimin Feng

Abstract

A novel 3D network Zn(Ⅱ) complex was synthesized in ethanol solvent,and was characterized by elemental analysis and IR.The crystal structure of Zn(Ⅱ) complex was also determined by X-ray single crystal diffraction.The results showed that this Zn(Ⅱ) complex was monoclinic,with unit cell C2/c and cell parameters:a=1.543 04(14) nm,b=1.271 50(11) nm,c=0.670 68(5) nm,V=1.286 61(19) nm3,Z=4,Mr=353.65,Dc=1.826 g/cm3,T=298(2) K,F(000)=720,μ(MoKα)=2.098 cm-1,R=0.022 9 and ωR=0.061 5.The compound formed 3D network structure through intermolecular hydrogen bonds and π-π interaction of pyridine rings.

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Key concepts: Chemistry, Monoclinic crystal system, Crystallography, Crystal structure, Hydrogen bond, Intermolecular force, Pyridine, Elemental analysis