2010•Journal of Weifang UniversityRequires access

Synthesis and Crystal Structure of 1D Chain Zn(II) Complex

Chu Si-yuan

Abstract

A novel 1D chain Zn(Ⅱ) complex was synthesized in CH3CH2OH solvent,and characterized by elemental analysis and IR.The crystal structure of Zn(Ⅱ) complex also has been determined by X-ray single crystal diffraction.The result shows it is monoclinic,space group Pc with a = 1.39761(14) nm,b = 2.3998(2) nm,c = 1.12395(12) nm,V = 3.5007(6) nm3,Z = 2,Mr = 1552.18,Dc = 1.473 g/cm3,T = 298(2) K,F(000) = 1620,μ(Mo Kα) = 0.772 cm-1,R = 0.1734 and ωR = 0.0409.The compound formed 1D chain structure through intermolecule and intramolecule hydrogen bonds and π-π interaction of pyridine rings.

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Key concepts: Monoclinic crystal system, Crystallography, Crystal structure, Hydrogen bond, Chemistry, Chain (unit), Pyridine, Single crystal