2014•Technology & Development of Chemical IndustryRequires access

Determination of Pyridine,Acrylonitrile in Water by Headspace Chromatography

Hu Ha

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Abstract

An analytical method for the pyridine and acrylonitrile in water by headspace chromatography was developed.Experimental parameters,included chromatographic conditions,headspace conditions,were optimized.The working curve of correlation coefficient was above 0.9995,the relative standard deviation was 1.9%,detection limit of pyridine and acrylonitrile was 0.05 mg/L and 0.01mg/L,respectively.The recovery of different types of water sample was 90.2%~100%.

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An analytical method for the pyridine and acrylonitrile in water by headspace chromatography was developed.Experimental parameters,included chromatographic conditions,headspace conditions,were optimized.The working curve of correlation coefficient was above 0.9995,the relative standard deviation was 1.9%,detection limit of pyridine and acrylonitrile was 0.05 mg/L and 0.01mg/L,respectively.The recovery of different types of water sample was 90.2%~100%.

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Available abstract

An analytical method for the pyridine and acrylonitrile in water by headspace chromatography was developed.Experimental parameters,included chromatographic conditions,headspace conditions,were optimized.The working curve of correlation coefficient was above 0.9995,the relative standard deviation was 1.9%,detection limit of pyridine and acrylonitrile was 0.05 mg/L and 0.01mg/L,respectively.The recovery of different types of water sample was 90.2%~100%.

Key concepts: Acrylonitrile, Pyridine, Chromatography, Chemistry, Relative standard deviation, Detection limit, Correlation coefficient, Standard curve

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