Synthesis and Structural Characterization of 2, 2-Bis (3-bromo-4-hydroxy-5-nitrophenyl) Propane
HU Yun-chu
Abstract
HU Yun-chu
Abstract
Using Bisphenol A as starting material, 2,2-Bis (3-bromo-4-hydroxy-5-nitrophenyl) propane was synthesized via nitration and bromation with the total yield of 83.1%. Its structure was certified by IR,~1HNMR,~(13) CNMR and MS after being cleaned by repeated crystallization.
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Using Bisphenol A as starting material, 2,2-Bis (3-bromo-4-hydroxy-5-nitrophenyl) propane was synthesized via nitration and bromation with the total yield of 83.1%. Its structure was certified by IR,~1HNMR,~(13) CNMR and MS after being cleaned by repeated crystallization.
Key concepts: Nitration, Propane, Yield (engineering), Characterization (materials science), Chemistry, Bisphenol A, Crystallization, Energetic material