2006•Chemical ResearchRequires access

Preparation of Cellulose Tri(4-methylbenzoate) Chiral Stationary Phases and Separation of Enantiomers

Guoxiang Li, Ping Ai, Lingling Zhou, Zhao Feng, Ding Hui, Li Li, Li‐Ming Yuan

Abstract

Cellulose tri(4-methylbenzoate)(CTMB) were synthesized,and coated on 3-aminopropyl silica gel.Their optical resolution abilities as chiral stationary phase(CSPs) were evaluated for high-performance liquid chromatography(HPLC).13 chiral compounds were resolved on the CSPs in the normal phase,and 9 chiral compounds could be separated.The CTMB CSPs show an excellent ability of resolving chiral compounds.

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Available abstract

Key concepts: Enantiomer, Chemistry, Chiral stationary phase, Cellulose, Chiral column chromatography, Chiral derivatizing agent, High-performance liquid chromatography, Chiral resolution