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The Study on Synthesis Teclmology of Ethyl Acetate Catalyzed by Sodium Bisulfate

Wei Chi

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Abstract

With sodium bisulfate as the catalyst,and acetic acid and alcohol as raw materials,ethyl acetate was synthesized.The effects of the reac- tion time,amount of catalyst,molar ratio of acid to alcohol and water carrying agent on esterification rate were discussed and the optimal reaction condi- tions were obtained as follows:based on 0.2 reel alcohol,the molar ratio of acetic acid to alcohol was 1.5:1,the amount of catalyst was 1.5 g,reaction time was 2h,and cyclohexane was 10 mL.Under these conditions,the highest yield of the reaction could reach 85.2%.Sodium bisulfate was a highly active catalyst for this reaction,le~ amount was required.And it was less pollution and contusion,cheap,the esterification rate was high and it could be recycled,so it had a good developing foreground.

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What this paper is about

With sodium bisulfate as the catalyst,and acetic acid and alcohol as raw materials,ethyl acetate was synthesized.The effects of the reac- tion time,amount of catalyst,molar ratio of acid to alcohol and water carrying agent on esterification rate were discussed and the optimal reaction condi- tions were obtained as follows:based on 0.2 reel alcohol,the molar ratio of acetic acid to alcohol was 1.5:1,the amount of catalyst was 1.5 g,reaction time was 2h,and cyclohexane was 10 mL.Under these conditions,the highest yield of the reaction could reach 85.2%.Sodium bisulfate was a highly active catalyst for this reaction,le~ amount was required.And it was less pollution and contusion,cheap,the esterification rate was high and it could be recycled,so it had a good developing foreground.

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Available abstract

With sodium bisulfate as the catalyst,and acetic acid and alcohol as raw materials,ethyl acetate was synthesized.The effects of the reac- tion time,amount of catalyst,molar ratio of acid to alcohol and water carrying agent on esterification rate were discussed and the optimal reaction condi- tions were obtained as follows:based on 0.2 reel alcohol,the molar ratio of acetic acid to alcohol was 1.5:1,the amount of catalyst was 1.5 g,reaction time was 2h,and cyclohexane was 10 mL.Under these conditions,the highest yield of the reaction could reach 85.2%.Sodium bisulfate was a highly active catalyst for this reaction,le~ amount was required.And it was less pollution and contusion,cheap,the esterification rate was high and it could be recycled,so it had a good developing foreground.

Key concepts: Catalysis, Acetic acid, Alcohol, Chemistry, Yield (engineering), Cyclohexane, Molar ratio, Sodium hypochlorite

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