Catalytic Synthesis of Butyl Acetate under Microwave Irradiation
Jun Wang
Abstract
Jun Wang
Abstract
The article researched that the esterification of acetic acid and n-butyl alcohol under the microwave radiation in reasonable power with iron trichloride as a catalyzer.And we have studied the optimum reaction term of it with the condition of microwave radiation:n(n-butanol)∶n(acid) 1.1∶1,mass of catalyst 0.3g, microwave radiation power 280W,the radiation time was only 8min, the yield was 89.2%.
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The article researched that the esterification of acetic acid and n-butyl alcohol under the microwave radiation in reasonable power with iron trichloride as a catalyzer.And we have studied the optimum reaction term of it with the condition of microwave radiation:n(n-butanol)∶n(acid) 1.1∶1,mass of catalyst 0.3g, microwave radiation power 280W,the radiation time was only 8min, the yield was 89.2%.
Key concepts: Catalysis, Acetic acid, Yield (engineering), Microwave, Alcohol, Microwave irradiation, Nuclear chemistry, Butanol