ScholarLens Back to search
2011•China Tea ProcessingRequires access

Determination of Imidacloprid Residue in Tea by SPE and GC-MS

Xiangzhen Liu

Open publisher page 0 citations

Abstract

Determination method of Imidacloprid residue in tea samples was developed.The Imidacloprid was extracted with acetonitrile in tea,then was purified with TPT SPE column,finally was detected by GC/MS.The limit of detection(LOD) was 4.00x10-12g,and the limit of quantitation(LOQ) of Imidacloprid in tea was 0.018mg/kg.At the range of 0.08~1.6mg/kg,the recovery rate of the method for Imidacloprid was between 85.27% and 95.88%.The variable coefficient was less than 8%.

About this research paper

What this paper is about

Determination method of Imidacloprid residue in tea samples was developed.The Imidacloprid was extracted with acetonitrile in tea,then was purified with TPT SPE column,finally was detected by GC/MS.The limit of detection(LOD) was 4.00x10-12g,and the limit of quantitation(LOQ) of Imidacloprid in tea was 0.018mg/kg.At the range of 0.08~1.6mg/kg,the recovery rate of the method for Imidacloprid was between 85.27% and 95.88%.The variable coefficient was less than 8%.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

Determination method of Imidacloprid residue in tea samples was developed.The Imidacloprid was extracted with acetonitrile in tea,then was purified with TPT SPE column,finally was detected by GC/MS.The limit of detection(LOD) was 4.00x10-12g,and the limit of quantitation(LOQ) of Imidacloprid in tea was 0.018mg/kg.At the range of 0.08~1.6mg/kg,the recovery rate of the method for Imidacloprid was between 85.27% and 95.88%.The variable coefficient was less than 8%.

Key concepts: Imidacloprid, Residue (chemistry), Detection limit, Chromatography, Chemistry, Gas chromatography–mass spectrometry, Pesticide, Mass spectrometry

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Determination of Imidacloprid Residue in Tea by SPE and GC-MS — Research Paper | ScholarLens