2006Biomass Chemical EngineeringRequires access

Study on Microwave-assisted Extraction of Yellow Pigment from Gardenia Jasminoiedes Ellis

LI Shen-zheng

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Abstract

The optimum technological parameters of microwave-assisted extraction of gardenia yellow pigment(GYP) were(studied.) An orthogonal test table L_9(3~4) was used with the factors of ethanol concentration,ratio of solid to liquid,power of(microwave) radiation and extracting time.The content of GYP was determined by spectrophotometry.The optimum conditions are as follows:(60 %) EtOH as extracting solvent,solid to liguid ratio 1 ∶20,power of microwave 280 W and extracting time 40 s.The extract yield was(17.83%) and extraction rate reached 98.20%.Compared with traditional methods such as leaching by water or organic solvents,it was proved that microwave-assisted extraction of GYP is a rapid method with higher yield.

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The optimum technological parameters of microwave-assisted extraction of gardenia yellow pigment(GYP) were(studied.) An orthogonal test table L_9(3~4) was used with the factors of ethanol concentration,ratio of solid to liquid,power of(microwave) radiation and extracting time.The content of GYP was determined by spectrophotometry.The optimum conditions are as follows:(60 %) EtOH as extracting solvent,solid to liguid ratio 1 ∶20,power of microwave 280 W and extracting time 40 s.The extract yield was(17.83%) and extraction rate reached 98.20%.Compared with traditional methods such as leaching by water or organic solvents,it was proved that microwave-assisted extraction of GYP is a rapid method with higher yield.

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Available abstract

The optimum technological parameters of microwave-assisted extraction of gardenia yellow pigment(GYP) were(studied.) An orthogonal test table L_9(3~4) was used with the factors of ethanol concentration,ratio of solid to liquid,power of(microwave) radiation and extracting time.The content of GYP was determined by spectrophotometry.The optimum conditions are as follows:(60 %) EtOH as extracting solvent,solid to liguid ratio 1 ∶20,power of microwave 280 W and extracting time 40 s.The extract yield was(17.83%) and extraction rate reached 98.20%.Compared with traditional methods such as leaching by water or organic solvents,it was proved that microwave-assisted extraction of GYP is a rapid method with higher yield.

Key concepts: Extraction (chemistry), Yield (engineering), Microwave, Chemistry, Chromatography, Pigment, Solvent, Leaching (pedology)

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