ScholarLens Back to search
2003•Fain kemikaruRequires access

Synthesis of 1H-1,2,3-Triazole under Microwave Irradiation

Wei Xu

Open publisher page 0 citations

Abstract

Starting with benzotriazole,1H1,2,3triazole was synthesized through two step reactions including oxidation by potassium permanganate and decarboxylation under microwave irradiation in overall yield of 647%.Compared with conventional method,in the decarboxylation reaction under microwave irradiation,the reaction time was reduced from 6 h to 6 min and the yield was enhanced from 65% to 97%.The product was corroborated by 1HNMR,13CNMR,IR and MS.

About this research paper

What this paper is about

Starting with benzotriazole,1H1,2,3triazole was synthesized through two step reactions including oxidation by potassium permanganate and decarboxylation under microwave irradiation in overall yield of 647%.Compared with conventional method,in the decarboxylation reaction under microwave irradiation,the reaction time was reduced from 6 h to 6 min and the yield was enhanced from 65% to 97%.The product was corroborated by 1HNMR,13CNMR,IR and MS.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

Starting with benzotriazole,1H1,2,3triazole was synthesized through two step reactions including oxidation by potassium permanganate and decarboxylation under microwave irradiation in overall yield of 647%.Compared with conventional method,in the decarboxylation reaction under microwave irradiation,the reaction time was reduced from 6 h to 6 min and the yield was enhanced from 65% to 97%.The product was corroborated by 1HNMR,13CNMR,IR and MS.

Key concepts: Decarboxylation, Yield (engineering), Potassium permanganate, Chemistry, Benzotriazole, Microwave irradiation, Irradiation, Microwave

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Synthesis of 1H-1,2,3-Triazole under Microwave Irradiation — Research Paper | ScholarLens