2002•Hecheng huaxueRequires access

Synthesis of n-Butyl Stearate Catalyzed by Ammonium Ferric Sulfate

Long Li-ping

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Abstract

n-Butyl stearate was synthesized in high yield by esterification of n-butyl alcohol with stearic acid in the presence of ammonium ferric sulfate dodecahydrate. The effects of the amount of ammonium ferric sulfate dodecahydrate, n-butyl alcohol and reaction time on the yield have been investigated. The yield of the ester could reache 98.8% under amount of substance ratio of stearic acid, n-butyl alcohol and ammonium ferric sulfate were 1∶8∶0.124, refluxing and water segregating for 2h.

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n-Butyl stearate was synthesized in high yield by esterification of n-butyl alcohol with stearic acid in the presence of ammonium ferric sulfate dodecahydrate. The effects of the amount of ammonium ferric sulfate dodecahydrate, n-butyl alcohol and reaction time on the yield have been investigated. The yield of the ester could reache 98.8% under amount of substance ratio of stearic acid, n-butyl alcohol and ammonium ferric sulfate were 1∶8∶0.124, refluxing and water segregating for 2h.

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Available abstract

n-Butyl stearate was synthesized in high yield by esterification of n-butyl alcohol with stearic acid in the presence of ammonium ferric sulfate dodecahydrate. The effects of the amount of ammonium ferric sulfate dodecahydrate, n-butyl alcohol and reaction time on the yield have been investigated. The yield of the ester could reache 98.8% under amount of substance ratio of stearic acid, n-butyl alcohol and ammonium ferric sulfate were 1∶8∶0.124, refluxing and water segregating for 2h.

Key concepts: Chemistry, Alcohol, Ferric, Stearic acid, Yield (engineering), Stearate, Sulfate, Ammonium sulfate

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