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Research on Synthetic Process of 1-Benzyl-4-piperidones

Lu Wen

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Abstract

Benzyl-4-piperidones, one of the important mid-body of OPC-21268, was synthesized from benzylamine and methyl acrylate. Process of every reaction was optimized, and the best condition of reaction was defined. The total yield of three reactions was 74.5%, which was 14.5% more than the yield reported in literature. The new process was fit to industry production for its easy method and low costs.

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What this paper is about

Benzyl-4-piperidones, one of the important mid-body of OPC-21268, was synthesized from benzylamine and methyl acrylate. Process of every reaction was optimized, and the best condition of reaction was defined. The total yield of three reactions was 74.5%, which was 14.5% more than the yield reported in literature. The new process was fit to industry production for its easy method and low costs.

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Available abstract

Benzyl-4-piperidones, one of the important mid-body of OPC-21268, was synthesized from benzylamine and methyl acrylate. Process of every reaction was optimized, and the best condition of reaction was defined. The total yield of three reactions was 74.5%, which was 14.5% more than the yield reported in literature. The new process was fit to industry production for its easy method and low costs.

Key concepts: Benzylamine, Yield (engineering), Process (computing), Acrylate, Methyl acrylate, Chemistry, Organic chemistry, Computer science

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