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Synthesis of Cyclohexyl Acetate Catalyzed by TiSiW_(12)O_(40)/TiO_2

Sun Ting

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Abstract

Cyclohexyl acetate was synthesized by esterification of acetic acid and cyclohexanol using TiSiW 12 O 40 /TiO 2 as a catalyst. Factors influencing the synthesis were discussed. The optimum conditions were as follows: the molar ratio of acetic acid to cyclohexanol is 1.0 ∶1.1, the amount of TiSiW 12 O 40 /TiO 2 is 5%(wt) of acetic acid; the reaction time is 1.5h. Under the optimum conditions the conversion of acetic acid is 95.5%.

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What this paper is about

Cyclohexyl acetate was synthesized by esterification of acetic acid and cyclohexanol using TiSiW 12 O 40 /TiO 2 as a catalyst. Factors influencing the synthesis were discussed. The optimum conditions were as follows: the molar ratio of acetic acid to cyclohexanol is 1.0 ∶1.1, the amount of TiSiW 12 O 40 /TiO 2 is 5%(wt) of acetic acid; the reaction time is 1.5h. Under the optimum conditions the conversion of acetic acid is 95.5%.

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Available abstract

Cyclohexyl acetate was synthesized by esterification of acetic acid and cyclohexanol using TiSiW 12 O 40 /TiO 2 as a catalyst. Factors influencing the synthesis were discussed. The optimum conditions were as follows: the molar ratio of acetic acid to cyclohexanol is 1.0 ∶1.1, the amount of TiSiW 12 O 40 /TiO 2 is 5%(wt) of acetic acid; the reaction time is 1.5h. Under the optimum conditions the conversion of acetic acid is 95.5%.

Key concepts: Cyclohexanol, Chemistry, Acetic acid, Catalysis, Molar ratio, Nuclear chemistry, Organic chemistry, Reaction conditions

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