2003•Chemical ResearchesRequires access

Preparation, Characterization, Crystal Structure of [(HOCH_2CH_2)_2NH_2]_6·P_2W_(18)O_(62)·6H_2O

Guo Dong

Abstract

A chargetransfer complex , \6·P2W18O62·6H2O, between the hertero polyacids H6P2W18O62·nH2O and the organic substrate diethanolamine, has been synthesized and characterized. The single crystal xray structure analysis of the title compund revealed that it belongs to R-3 space group, a=b=c=1.362 98(16)nm, α=β=γ=106.490(17)°, Z=1, V=2.137 4(4) nm3, R=0.083 7, Rw=0.221 9.

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Key concepts: Diethanolamine, Crystal structure, Crystallography, Crystal (programming language), Chemistry, Single crystal, Substrate (aquarium), Stereochemistry