2004•Chemical ResearchesRequires access
Synthesis and Crystal Structure of a New Isopolycompound[C_6H_5CH_2NH(CH_3)_2]_4[Mo_8O_(26)]·4H_2O
Duan Xianying
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Abstract
A new compound \_4\·4H_2O was synthesized from MoO_3 and C_6H_5CH_2N(CH_3)_2, and crystallized by diffusion. Single crystal X-ray analysis indicates that the title compound belongs to triclinic system, space group Pī, crystal cell parameter a=1.068 5(2) nm, b=1.405 0(3) nm, c= 1.064 3(2) nm, α= 93.12(3)°, β= 110.26(3)°, γ= 71.41(3)°, V=(1.417 9(5)) nm~3, R=0.038 3.