2004•Unpublished venueRequires access

Preparation of cyclohexene by catalyzed dehydration of cyclohexanol by SnCl_4·5H_2O under microwave irradiation

Xian‐You Yuan

Abstract

Preparation of cyclohexene by catalyzed dehydration of cyclohexanol by SnCl4·5H2O under microwave irradiation was studied.The influences of catalyst amount,microwave irradiation power and time on the reaction were investigated.Thee most suitable conditions for the reaction were as follows: cyclohexanol 10mL, SnCl4·5H2O 2g, microwave irradiation power 600W,time 10 min.The yield was up to 68.4%.

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Key concepts: Cyclohexanol, Cyclohexene, Microwave irradiation, Catalysis, Dehydration, Irradiation, Chemistry, Yield (engineering)