Study on Chemical Constituents of Semen Pharbitidis(II)
Ping Li
Abstract
Ping Li
Abstract
The active constituents in semen pharbitidis were studied.Seperation and purification were performed on columns of silica gel and Sephadex LH-20,and the chemical structures were elucidated by various spectroscopic data.Eight compounds were isolated from ethyl acetate fraction of 70 %(volume fraction) ethanol extract,and identified as cinnamic acid(Ⅰ),ferulic acid(Ⅱ),chlorogenic acid(Ⅲ),methyl chloroformate(Ⅳ),propyl chloroformate(Ⅴ),rhein(Ⅵ),12-hydroxy-methyl abieformate(Ⅶ) and 12-hydroxy-hydromethylabieformate(Ⅷ).These compounds were isolated from the genus Pharbitis for the first time by search.
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The active constituents in semen pharbitidis were studied.Seperation and purification were performed on columns of silica gel and Sephadex LH-20,and the chemical structures were elucidated by various spectroscopic data.Eight compounds were isolated from ethyl acetate fraction of 70 %(volume fraction) ethanol extract,and identified as cinnamic acid(Ⅰ),ferulic acid(Ⅱ),chlorogenic acid(Ⅲ),methyl chloroformate(Ⅳ),propyl chloroformate(Ⅴ),rhein(Ⅵ),12-hydroxy-methyl abieformate(Ⅶ) and 12-hydroxy-hydromethylabieformate(Ⅷ).These compounds were isolated from the genus Pharbitis for the first time by search.
Key concepts: Chemistry, Sephadex, Ethyl chloroformate, Ethyl acetate, Chromatography, Ferulic acid, Silica gel, Ethanol