Chemical Constituents from Lythrum salicaria L.
Bei Jiang
Abstract
Bei Jiang
Abstract
OBJECTIVE To investigate the chemical constituents from the stems of Lythrum salicaria L.. METHODS The constituents were isolated and purified by silica gel,Sephadex LH- 20 column chromatography,and TLC. The structures were identified on the basis of spectral data and physiochemical characteristics. RESULTS Twenty compounds were isolated from 70% ethanol extracts and identified as betulinic acid( 1),2α,3α,24-trihydroxy-12( 13)-en-urs-28-oic acid( 2),6-O-( E)- sinapoylpoligalitol( 3),feruloyl-6'-O-α-D-glucopyranoside( 4),7-oxo-β-sitosterol( 5),en-tisolariciresinol( 6),muramine( 7),aesculetin( 8),apigenin( 9),( 2E,6S)-2,6-dimethyl-6-O-β-D-xylpyranosyloxy-2,7-menthiafolic acid( 10), quercetin3-O-( 6″-caffeoyl)-β-D-galactopyranoside( 11),cycloart-23-ene-3β,25-diol( 12),( 1'S,6'R)-8'-hydroxyabscisic acid-β-D-glucoside( 13),3',5-dihydroxy-3,6,4'-trimethoxyl-7-O-β-D-glucopyranoside flavonoid( 14),aurantiamide acetate( 15),5,6,3',4'-tetrahydroxy-3,7-dimethoxy-flavone( 16),ursolic acid( 17),oleanolic acid( 18),4-O-11-methyl-oleoside-p-hydroxyphenyl-( 6'-11-methyloleoside)-β-D-glucopyranoside( 19),and 6-O-galloylarbutin( 20). CONCLUSION Except for compounds 8 and 9,all the compounds were isolated from this plant material for the first time.
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OBJECTIVE To investigate the chemical constituents from the stems of Lythrum salicaria L.. METHODS The constituents were isolated and purified by silica gel,Sephadex LH- 20 column chromatography,and TLC. The structures were identified on the basis of spectral data and physiochemical characteristics. RESULTS Twenty compounds were isolated from 70% ethanol extracts and identified as betulinic acid( 1),2α,3α,24-trihydroxy-12( 13)-en-urs-28-oic acid( 2),6-O-( E)- sinapoylpoligalitol( 3),feruloyl-6'-O-α-D-glucopyranoside( 4),7-oxo-β-sitosterol( 5),en-tisolariciresinol( 6),muramine( 7),aesculetin( 8),apigenin( 9),( 2E,6S)-2,6-dimethyl-6-O-β-D-xylpyranosyloxy-2,7-menthiafolic acid( 10), quercetin3-O-( 6″-caffeoyl)-β-D-galactopyranoside( 11),cycloart-23-ene-3β,25-diol( 12),( 1'S,6'R)-8'-hydroxyabscisic acid-β-D-glucoside( 13),3',5-dihydroxy-3,6,4'-trimethoxyl-7-O-β-D-glucopyranoside flavonoid( 14),aurantiamide acetate( 15),5,6,3',4'-tetrahydroxy-3,7-dimethoxy-flavone( 16),ursolic acid( 17),oleanolic acid( 18),4-O-11-methyl-oleoside-p-hydroxyphenyl-( 6'-11-methyloleoside)-β-D-glucopyranoside( 19),and 6-O-galloylarbutin( 20). CONCLUSION Except for compounds 8 and 9,all the compounds were isolated from this plant material for the first time.
Key concepts: Betulinic acid, Oleanolic acid, Sephadex, Chemistry, Ursolic acid, Apigenin, Column chromatography, Flavonoid