Determination of Danshensu in Jiakangling Granules by HPLC
Gao Ya-xiong
Abstract
Gao Ya-xiong
Abstract
Objective To determine Danshensu in Jiakangling Granules by HPLC.Methods HPLC analysis was applied to determine Danshensu in Jiakangling Granules.The HPLC chromatographic conditions included Hypersil BDS column;the mobile phase was methanol-1% glacial acetic(10:90)and the detective wavelength was at 280 nm,column temperature was 25℃.Results There were good linear relationship for Danshensu within the range of 3.612-18.06 μg/ml,r=0.999 9.The average recovery was 98.9%,RSD=1.7%(n=5).Conclusion The methods were of good accurate and a simple procedure.It may be practical to control the quality of Jiakangling Granules.
A significance statement is not available in the OpenAlex record.
A contribution statement is not available in the OpenAlex record.
Method details are not available in the OpenAlex metadata.
Findings are not separately available in the OpenAlex metadata.
Limitations are not available in the OpenAlex metadata.
Application details are not available in the OpenAlex metadata.
Objective To determine Danshensu in Jiakangling Granules by HPLC.Methods HPLC analysis was applied to determine Danshensu in Jiakangling Granules.The HPLC chromatographic conditions included Hypersil BDS column;the mobile phase was methanol-1% glacial acetic(10:90)and the detective wavelength was at 280 nm,column temperature was 25℃.Results There were good linear relationship for Danshensu within the range of 3.612-18.06 μg/ml,r=0.999 9.The average recovery was 98.9%,RSD=1.7%(n=5).Conclusion The methods were of good accurate and a simple procedure.It may be practical to control the quality of Jiakangling Granules.
Key concepts: Chromatography, High-performance liquid chromatography, Chemistry, Granule (geology), Materials science, Composite material