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Determination of Nickel Content in Catalyst by Air-Acetylene Flame Atomic Absorption Spectrometry

Yang Wen-sheng

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Abstract

The method of determining nickel content in catalyst by air-acetylene flame atomic absorption spectrometry was studied. The samples were digested in pressure digestion, and the solvent was aquaregia. It had advantages that the amount of reagent was a little and pollution was little, The RSD of the method were less than 2.0 %( n =8),and the recoveries were between 97.3 %~102 %.

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The method of determining nickel content in catalyst by air-acetylene flame atomic absorption spectrometry was studied. The samples were digested in pressure digestion, and the solvent was aquaregia. It had advantages that the amount of reagent was a little and pollution was little, The RSD of the method were less than 2.0 %( n =8),and the recoveries were between 97.3 %~102 %.

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Available abstract

The method of determining nickel content in catalyst by air-acetylene flame atomic absorption spectrometry was studied. The samples were digested in pressure digestion, and the solvent was aquaregia. It had advantages that the amount of reagent was a little and pollution was little, The RSD of the method were less than 2.0 %( n =8),and the recoveries were between 97.3 %~102 %.

Key concepts: Atomic absorption spectroscopy, Reagent, Acetylene, Catalysis, Nickel, Chemistry, Analytical Chemistry (journal), Microwave digestion

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