Researches on Analysis Method of N-acetyl H Acid' Contents
Fan Li
Abstract
Fan Li
Abstract
Analyzed the influence of the adding quantity of the sulfuric acid and the reaction time to N-acetyl H acid hydrolysis degree.Under the backflow condition,N-acetyl H acid(wet) 10g,water 100mL,experiment obtained the best hydrolisis condition of N-acetyl H acid completely hydrolisis to H acid and acetic acid.The optimum conditions is sulfuric acid recruitment 10mL and hydrolisis time 1h.And calculated the N-acetyl H acid content with the aid of diazotization analytical method.
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Analyzed the influence of the adding quantity of the sulfuric acid and the reaction time to N-acetyl H acid hydrolysis degree.Under the backflow condition,N-acetyl H acid(wet) 10g,water 100mL,experiment obtained the best hydrolisis condition of N-acetyl H acid completely hydrolisis to H acid and acetic acid.The optimum conditions is sulfuric acid recruitment 10mL and hydrolisis time 1h.And calculated the N-acetyl H acid content with the aid of diazotization analytical method.
Key concepts: Sulfuric acid, Hydrolysis, Acetic acid, Chemistry, Backflow, Acid hydrolysis, Chromatography, Nuclear chemistry