2009•Zhongguo yaowu huaxue zazhiRequires access

Lipophilic compounds of Callicarpa nudiflora Hook. Et Arn.

Jinhui Wang

Open publisher page 11 citations

Abstract

Aim To study the lipophilic compounds of the leaves of Callicarpa nudiflora Hook.Et Arn.Methods This compounds were isolated by column chromatography on silica gel,Sephadex LH-20 and HPD-100 macroporous resin,and their structures were identified by physicochemical and spectral data.Results Eight compounds were obtained and identified as 5,4'-dihydroxy-3,7,3'-trimethoxyflavone(1),5-hydroxy-3,7,3',4'-tetramethoxyflavone(2),luteolin(3),luteolin-7-O-β-D-glucopyranoside(4),aesculetin(5),urs-12-en-3β-ol(6),ursolic acid(7),β-sitosterol(8).Conclusion Compounds 5,6 were isolated from Callicarpa genus for the first time.Compounds 1-3,8 were isolated from this plant for the first time.The coumarins was firstly obtained from the genus.

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Aim To study the lipophilic compounds of the leaves of Callicarpa nudiflora Hook.Et Arn.Methods This compounds were isolated by column chromatography on silica gel,Sephadex LH-20 and HPD-100 macroporous resin,and their structures were identified by physicochemical and spectral data.Results Eight compounds were obtained and identified as 5,4'-dihydroxy-3,7,3'-trimethoxyflavone(1),5-hydroxy-3,7,3',4'-tetramethoxyflavone(2),luteolin(3),luteolin-7-O-β-D-glucopyranoside(4),aesculetin(5),urs-12-en-3β-ol(6),ursolic acid(7),β-sitosterol(8).Conclusion Compounds 5,6 were isolated from Callicarpa genus for the first time.Compounds 1-3,8 were isolated from this plant for the first time.The coumarins was firstly obtained from the genus.

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Available abstract

Aim To study the lipophilic compounds of the leaves of Callicarpa nudiflora Hook.Et Arn.Methods This compounds were isolated by column chromatography on silica gel,Sephadex LH-20 and HPD-100 macroporous resin,and their structures were identified by physicochemical and spectral data.Results Eight compounds were obtained and identified as 5,4'-dihydroxy-3,7,3'-trimethoxyflavone(1),5-hydroxy-3,7,3',4'-tetramethoxyflavone(2),luteolin(3),luteolin-7-O-β-D-glucopyranoside(4),aesculetin(5),urs-12-en-3β-ol(6),ursolic acid(7),β-sitosterol(8).Conclusion Compounds 5,6 were isolated from Callicarpa genus for the first time.Compounds 1-3,8 were isolated from this plant for the first time.The coumarins was firstly obtained from the genus.

Key concepts: Chemistry, Luteolin, Ursolic acid, Sephadex, Column chromatography, Silica gel, Chromatography, Stereochemistry

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