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2004•Journal of Henan Institute of EducationRequires access

Preparation and Application of Cellulose Tribenzoate Chiral Column

Hu Xiao

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Abstract

Cellulose tribenzoate(CTB) was synthesized for the coating of high performance liquid chromatographic stationary phases Elemental analysis and IR spectra indicated that most of the hydroxy groups of the microcrystalline cellulose had been converted into ester groups The evaluation of column was achieved hexane/2-propanol(90∶10 v/v) as mobile phase at a flow rate of 1ml·min -1 (at25℃) And the results of the separation of chiral compound showed that the chiral stationary has good steroelectivity

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What this paper is about

Cellulose tribenzoate(CTB) was synthesized for the coating of high performance liquid chromatographic stationary phases Elemental analysis and IR spectra indicated that most of the hydroxy groups of the microcrystalline cellulose had been converted into ester groups The evaluation of column was achieved hexane/2-propanol(90∶10 v/v) as mobile phase at a flow rate of 1ml·min -1 (at25℃) And the results of the separation of chiral compound showed that the chiral stationary has good steroelectivity

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Available abstract

Cellulose tribenzoate(CTB) was synthesized for the coating of high performance liquid chromatographic stationary phases Elemental analysis and IR spectra indicated that most of the hydroxy groups of the microcrystalline cellulose had been converted into ester groups The evaluation of column was achieved hexane/2-propanol(90∶10 v/v) as mobile phase at a flow rate of 1ml·min -1 (at25℃) And the results of the separation of chiral compound showed that the chiral stationary has good steroelectivity

Key concepts: Microcrystalline cellulose, Cellulose, Chromatography, Hexane, Volumetric flow rate, Chemistry, Microcrystalline, Phase (matter)

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