Chemical constituents of Bidens bipinnata (II)
Shuai Li, Kuang Haixue AYoshihito Okada, Toru Okuyama
Abstract
Shuai Li, Kuang Haixue AYoshihito Okada, Toru Okuyama
Abstract
Object To study the chemical constituents of Bidens bipinnata L Methods Isolation and purification were carried out on silica gel, ODS column, and Sephadex LH 20, HPLC, identified by physicochemical properties and structurally elucidated by spectral analysis Results From n BuOH extract of B bipinnata, 12 compounds were obtained and identified as: 6 O β D glucopyranosyl 6, 7, 3′, 4′ tetrahydroxyaurone (Ⅰ), 6 O (6″ acetyl β D glucopyranosyl) 6, 7, 3′, 4′ tetrahydroxyaurone (Ⅱ), quercetin 3 O β D glucopyranoside (Ⅲ), quercetin 3 O α L rhamnoside (Ⅳ), iso okanin 7 O β D glucopyranoside (Ⅴ), esculin (Ⅵ), (E) 2 hexenyl O β D glucopyranoside (Ⅶ), n hexyl O β D glucopyranoside (Ⅷ), isopentyl O β D glucopyranoside (Ⅸ), n butyl O α D fructofuranoside (Ⅹ), n butyl O β D fructofuranoside (Ⅺ), n butyl O β D fructopyranoside ( ⅩⅡ ) Conclusion All of these compounds, except Ⅰ and Ⅴ, are obtained from the plant for the first time
OpenAlex reports 8 citations for this work. Citation counts describe recorded attention and do not establish research quality.
A contribution statement is not available in the OpenAlex record.
Method details are not available in the OpenAlex metadata.
Findings are not separately available in the OpenAlex metadata.
Limitations are not available in the OpenAlex metadata.
Application details are not available in the OpenAlex metadata.
Object To study the chemical constituents of Bidens bipinnata L Methods Isolation and purification were carried out on silica gel, ODS column, and Sephadex LH 20, HPLC, identified by physicochemical properties and structurally elucidated by spectral analysis Results From n BuOH extract of B bipinnata, 12 compounds were obtained and identified as: 6 O β D glucopyranosyl 6, 7, 3′, 4′ tetrahydroxyaurone (Ⅰ), 6 O (6″ acetyl β D glucopyranosyl) 6, 7, 3′, 4′ tetrahydroxyaurone (Ⅱ), quercetin 3 O β D glucopyranoside (Ⅲ), quercetin 3 O α L rhamnoside (Ⅳ), iso okanin 7 O β D glucopyranoside (Ⅴ), esculin (Ⅵ), (E) 2 hexenyl O β D glucopyranoside (Ⅶ), n hexyl O β D glucopyranoside (Ⅷ), isopentyl O β D glucopyranoside (Ⅸ), n butyl O α D fructofuranoside (Ⅹ), n butyl O β D fructofuranoside (Ⅺ), n butyl O β D fructopyranoside ( ⅩⅡ ) Conclusion All of these compounds, except Ⅰ and Ⅴ, are obtained from the plant for the first time
Key concepts: Chemistry, Sephadex, Quercetin, Chromatography, Silica gel, Column chromatography, High-performance liquid chromatography, Organic chemistry