Synthesis of Butyl Butyrate Catalyzed by Sodium Bisulfate
Song Xiao
Abstract
Song Xiao
Abstract
The butyl butyrate were synthesized by the esterification reaction of butyric acid and butanol catalyzed by sodium bisulfate.The effects of reaction time,amount of catalyst,acid/alcohol molar ratio on esterification conversion were discussed and the optimal reaction conditions were obtained:acid/alcohol molar ratio 1∶1.1,amount of sodium bisulfate 0.1 g,reaction time 60 min,reaction temperature 120~140 ℃,the esterification ratio more than 98 8%.
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The butyl butyrate were synthesized by the esterification reaction of butyric acid and butanol catalyzed by sodium bisulfate.The effects of reaction time,amount of catalyst,acid/alcohol molar ratio on esterification conversion were discussed and the optimal reaction conditions were obtained:acid/alcohol molar ratio 1∶1.1,amount of sodium bisulfate 0.1 g,reaction time 60 min,reaction temperature 120~140 ℃,the esterification ratio more than 98 8%.
Key concepts: Molar ratio, Chemistry, Alcohol, Catalysis, Butyric acid, Sodium, Reaction conditions, Butanol