2010Chinese Journal of Spectroscopy LaboratoryRequires access

Determination of Seven Trace Elements in Bamboo Shoots by Microwave Digestion ICP-MS

Yong Yue

Open publisher page 0 citations

Abstract

A method for simultaneous analysis of seven elements (Cr,Cu,Zn,As,Cd,Hg,Pb) in bamboo shoot were established.The samples were pretreated through microwave digestion system with nitric acid solution,and then determined by inductively coupled plasma-mass spectrometry (ICP-MS).A good linearity of calibration curves was obtained,the correlative coefficients were 0.9937—1.0000.The limits of detection were between 0.005μg/L and 0.202μg/L.The average spiked recoveries ranged from 88.96% to 110.5%.RSD was less than 6.09% and the analytical results of national tomato leaf standard(GSBZ 51001-94)showed acceptable agreement with the certified values.This method is sensitive,reliable,rapid and accurate for the multi-elements determination of bamboo shoot by ICP-MS.

About this research paper

What this paper is about

A method for simultaneous analysis of seven elements (Cr,Cu,Zn,As,Cd,Hg,Pb) in bamboo shoot were established.The samples were pretreated through microwave digestion system with nitric acid solution,and then determined by inductively coupled plasma-mass spectrometry (ICP-MS).A good linearity of calibration curves was obtained,the correlative coefficients were 0.9937—1.0000.The limits of detection were between 0.005μg/L and 0.202μg/L.The average spiked recoveries ranged from 88.96% to 110.5%.RSD was less than 6.09% and the analytical results of national tomato leaf standard(GSBZ 51001-94)showed acceptable agreement with the certified values.This method is sensitive,reliable,rapid and accurate for the multi-elements determination of bamboo shoot by ICP-MS.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

A method for simultaneous analysis of seven elements (Cr,Cu,Zn,As,Cd,Hg,Pb) in bamboo shoot were established.The samples were pretreated through microwave digestion system with nitric acid solution,and then determined by inductively coupled plasma-mass spectrometry (ICP-MS).A good linearity of calibration curves was obtained,the correlative coefficients were 0.9937—1.0000.The limits of detection were between 0.005μg/L and 0.202μg/L.The average spiked recoveries ranged from 88.96% to 110.5%.RSD was less than 6.09% and the analytical results of national tomato leaf standard(GSBZ 51001-94)showed acceptable agreement with the certified values.This method is sensitive,reliable,rapid and accurate for the multi-elements determination of bamboo shoot by ICP-MS.

Key concepts: Microwave digestion, Nitric acid, Inductively coupled plasma mass spectrometry, Chemistry, Detection limit, Calibration curve, Chromatography, Analytical Chemistry (journal)

Related papers

Back to paper searchBrowse research topicsOriginal source
Determination of Seven Trace Elements in Bamboo Shoots by Microwave Digestion ICP-MS — Research Paper | ScholarLens