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X-Ray Powder Diffraction and IR Study of Calcium Borophosphate CaBPO5

A. Baykal, G. Gözel, M. Kızılyallı, Muhammet S. Toprak, Rüdiger Kniep

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Abstract

In this study, CaBPO5 was synthesized by different solid state reactions than reported before and its X-ray powder diffraction and IR data were reported. In one of these solid state reactions BPO4 was used as a phosphating agent. The examination of the X-ray powder diffraction data showed that this compound crystallized in a hexagonal system and the refined unit cell parameters were a = 6.684, c = 6.616(2) \\AA, with Z=3 as reported before. From the observed reflections, the space group was determined as P3121, and its density was found to be 3.15 g/cc. The X-ray powder diffraction and IR data, which were in agreement with the reported crystal structure, are given the first time in this work.

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What this paper is about

In this study, CaBPO5 was synthesized by different solid state reactions than reported before and its X-ray powder diffraction and IR data were reported. In one of these solid state reactions BPO4 was used as a phosphating agent. The examination of the X-ray powder diffraction data showed that this compound crystallized in a hexagonal system and the refined unit cell parameters were a = 6.684, c = 6.616(2) \\AA, with Z=3 as reported before. From the observed reflections, the space group was determined as P3121, and its density was found to be 3.15 g/cc. The X-ray powder diffraction and IR data, which were in agreement with the reported crystal structure, are given the first time in this work.

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Available abstract

In this study, CaBPO5 was synthesized by different solid state reactions than reported before and its X-ray powder diffraction and IR data were reported. In one of these solid state reactions BPO4 was used as a phosphating agent. The examination of the X-ray powder diffraction data showed that this compound crystallized in a hexagonal system and the refined unit cell parameters were a = 6.684, c = 6.616(2) \\AA, with Z=3 as reported before. From the observed reflections, the space group was determined as P3121, and its density was found to be 3.15 g/cc. The X-ray powder diffraction and IR data, which were in agreement with the reported crystal structure, are given the first time in this work.

Key concepts: Chemistry, Powder diffraction, Solid-state, Diffraction, X-ray crystallography, Calcium, Crystallography, X-ray

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X-Ray Powder Diffraction and IR Study of Calcium Borophosphate CaBPO5 — Research Paper | ScholarLens