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Synthesis of Strontium Borophosphate, SrBPO5 by Solid State and Hydrothermal Methods and Characterisation

A. Baykal, M. Kızılyallı, G. Gözel, Rüdiger Kniep

Open publisher page 29 citations

Abstract

SrBPO5 was synthesized by a solid-state reaction reported and by a new solid state reaction using BPO4 as a phosphating agent. It was also obtained by a hydrothermal method. The structure of the compound was solved by Rietveld analysis before. The examination of X-ray powder diffraction data showed that, SrBPO5 is isostructural with CaBPO5 and BaBPO5. It crystallizes in the trigonal system in P3121 and the refined unit cell parameters are a = 6.8488(1), c = 6.8159(2) Å, Z=3 and Dm 3.77 g/cm3.

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What this paper is about

SrBPO5 was synthesized by a solid-state reaction reported and by a new solid state reaction using BPO4 as a phosphating agent. It was also obtained by a hydrothermal method. The structure of the compound was solved by Rietveld analysis before. The examination of X-ray powder diffraction data showed that, SrBPO5 is isostructural with CaBPO5 and BaBPO5. It crystallizes in the trigonal system in P3121 and the refined unit cell parameters are a = 6.8488(1), c = 6.8159(2) Å, Z=3 and Dm 3.77 g/cm3.

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Available abstract

SrBPO5 was synthesized by a solid-state reaction reported and by a new solid state reaction using BPO4 as a phosphating agent. It was also obtained by a hydrothermal method. The structure of the compound was solved by Rietveld analysis before. The examination of X-ray powder diffraction data showed that, SrBPO5 is isostructural with CaBPO5 and BaBPO5. It crystallizes in the trigonal system in P3121 and the refined unit cell parameters are a = 6.8488(1), c = 6.8159(2) Å, Z=3 and Dm 3.77 g/cm3.

Key concepts: Isostructural, Hydrothermal circulation, Strontium, Solid-state, Rietveld refinement, Hydrothermal synthesis, Trigonal crystal system, Powder diffraction

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