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2021•International Journal of Pharmacy and Pharmaceutical ScienceOpen access

Determination of lornoxicam by UV spectroscopic method in bulk and combined dosage form

Shoaeb Mohammad Syed, Vikas Rajurkar, RAJENDRA P. MARATHE

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Abstract

Objective: In the present study a suitable UV Spectroscopic method was developed and validated for Lornoxicam determination in bulk and combined dosage form. Methods: UV Spectrophotometric method was performed at 376nm and samples were prepared with a solution of 0.1N HCl, validation parameters like accuracy, precision, LOD, LOQ, recovery study and range were determined. Results: The linearity demonstrated a correlation coefficient of 0.9992 various validation parameters like accuracy, precision, LOD, LOQ, recovery study and range were found to be within the specified range. Conclusion: The proposed method was simple, rapid, precise, accurate and sensitive and can be used for routine analysis of Lornoxicam in bulk and combined dosage form.

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Objective: In the present study a suitable UV Spectroscopic method was developed and validated for Lornoxicam determination in bulk and combined dosage form. Methods: UV Spectrophotometric method was performed at 376nm and samples were prepared with a solution of 0.1N HCl, validation parameters like accuracy, precision, LOD, LOQ, recovery study and range were determined. Results: The linearity demonstrated a correlation coefficient of 0.9992 various validation parameters like accuracy, precision, LOD, LOQ, recovery study and range were found to be within the specified range. Conclusion: The proposed method was simple, rapid, precise, accurate and sensitive and can be used for routine analysis of Lornoxicam in bulk and combined dosage form.

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Available abstract

Objective: In the present study a suitable UV Spectroscopic method was developed and validated for Lornoxicam determination in bulk and combined dosage form. Methods: UV Spectrophotometric method was performed at 376nm and samples were prepared with a solution of 0.1N HCl, validation parameters like accuracy, precision, LOD, LOQ, recovery study and range were determined. Results: The linearity demonstrated a correlation coefficient of 0.9992 various validation parameters like accuracy, precision, LOD, LOQ, recovery study and range were found to be within the specified range. Conclusion: The proposed method was simple, rapid, precise, accurate and sensitive and can be used for routine analysis of Lornoxicam in bulk and combined dosage form.

Key concepts: Lornoxicam, Correlation coefficient, Accuracy and precision, Linearity, Dosage form, Chromatography, Materials science, Chemistry

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