2009•Xiandai shipin kejiRequires access
Determination of aluminum in aquatic product by graphite furnace atomic absorption spectrometry with microwave digestion.
Jie Sun, Zhu Jia, Ling Qiao, Xu Hua
Open publisher page 0 citations
Abstract
A novel method for determination of aluminum in aquatic products was developed in this paper. The sample was dissolved with microwave digestion and determined by graphite furnace atomic absorption spectrometry. 0.3% Mg(NO3)2 and 0.1% Pd(NO3)2-0.3% Mg(NO3)2-1.0% NH4H2PO4 were chosen as matrix modifier. Results showed that the best matrix modifier, pyrolysis temperatures and atomization temperature were 0.1%Pd(NO3)2 -0.3%Mg(NO3)2-1.0% NH4H2PO4, 1300 ℃ and 2350 ℃, respectively. The detection limit, RSD and recovery rate of the method were 2.08 μg/L, 2.44%-6.81%, and 94.10%-107.95%, respectively. The method was fast and effective for detection of aluminum content in aquatic products.