Catalytic Synthesis of Benzaldehyde Glycol Acetal over H_3PW_6Mo_6O_(40)/PAn
Fei Gao
Abstract
Fei Gao
Abstract
H_3PW_6Mo_6O_40/PAn was used as catalyst for synthesizing benzaldehyde glycol acetal from benzaldehyde and glycol.Under the optimum conditions,that the molar ratio of benzaldehyde to glycol is 1/1.4,the mass ratio of the catalyst to the reactants is 0.8%,and the reaction time is 45 min,the yield of benzaldehyde glycol acetal is 79.0%.This catalyst has many advantages,such as low catalyst dosage,short reaction time,high activity and pollution-free to the environment.
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H_3PW_6Mo_6O_40/PAn was used as catalyst for synthesizing benzaldehyde glycol acetal from benzaldehyde and glycol.Under the optimum conditions,that the molar ratio of benzaldehyde to glycol is 1/1.4,the mass ratio of the catalyst to the reactants is 0.8%,and the reaction time is 45 min,the yield of benzaldehyde glycol acetal is 79.0%.This catalyst has many advantages,such as low catalyst dosage,short reaction time,high activity and pollution-free to the environment.
Key concepts: Benzaldehyde, Acetal, Catalysis, Yield (engineering), Chemistry, Molar ratio, Organic chemistry, Nuclear chemistry