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2021•Transactions of the Materials Research Society of JapanOpen access

Syntheses and Structures of Keggin-Type Polyoxometalate Crystals Hybridized with a Polymerizable Ionic-Liquid

Saki Otobe, Yoshiki Kiyota, Tatsuhiro Kojima, Yoshiki Oda, Shinichi Koguchi, Yosuke Okamura, Masashi Higuchi, Masaki Kawano, Yu Nagase, Takeru Ito

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Abstract

Keggin-type polyoxometalate clusters were successfully hybridized with a polymerizable ionic-liquid having methacryloyl group and imidazolium moieties (denoted as MAImC1). Metatungstate ([H2W12O40]6−, H2W12) and dodecamolybdophosphate ([PMo12O40]3−, PMo12) anions were firstly employed to obtain inorganic-organic hybrid crystals. Their compositions and structures were clearly revealed by single crystal structure analyses.

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Keggin-type polyoxometalate clusters were successfully hybridized with a polymerizable ionic-liquid having methacryloyl group and imidazolium moieties (denoted as MAImC1). Metatungstate ([H2W12O40]6−, H2W12) and dodecamolybdophosphate ([PMo12O40]3−, PMo12) anions were firstly employed to obtain inorganic-organic hybrid crystals. Their compositions and structures were clearly revealed by single crystal structure analyses.

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Available abstract

Keggin-type polyoxometalate clusters were successfully hybridized with a polymerizable ionic-liquid having methacryloyl group and imidazolium moieties (denoted as MAImC1). Metatungstate ([H2W12O40]6−, H2W12) and dodecamolybdophosphate ([PMo12O40]3−, PMo12) anions were firstly employed to obtain inorganic-organic hybrid crystals. Their compositions and structures were clearly revealed by single crystal structure analyses.

Key concepts: Polyoxometalate, Ionic liquid, Ionic bonding, Keggin structure, Ionic crystal, Crystallography, Type (biology), Crystal structure

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