Synthesis of β-Naphthol Ethyl Ether Using Polyethylene Glycol as a Phase Transfer Catalyst
Hongqing Xiao
Abstract
Hongqing Xiao
Abstract
β-Naphthol ethyl ether was prepared by the reaction of β-naphthol with bromic ether in the presence of polyethylene glycol.The effect of different factors such as the amount of catalyst,the molar ratio of β-naphthol to bromic ether,reaction time and etc.on yield of β-naphthol ethyl ether was carefully studied.When the molar ratio of β-naphthol to bromic ether was 1∶1 and the reaction time was 1.7 h,the yield of β-naphthol ethyl ether was 95.4%.
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β-Naphthol ethyl ether was prepared by the reaction of β-naphthol with bromic ether in the presence of polyethylene glycol.The effect of different factors such as the amount of catalyst,the molar ratio of β-naphthol to bromic ether,reaction time and etc.on yield of β-naphthol ethyl ether was carefully studied.When the molar ratio of β-naphthol to bromic ether was 1∶1 and the reaction time was 1.7 h,the yield of β-naphthol ethyl ether was 95.4%.
Key concepts: Chemistry, Ether, Polyethylene glycol, Yield (engineering), Catalysis, Organic chemistry, Molar ratio, 1-Naphthol