2011•Science & Technology in Chemical IndustryRequires access
Synthesis of higher alcohol
Shuang Zhang
Open publisher page 0 citations
Abstract
Using paraffin and boric acid as raw material for the first time,boric acid ester was synthesized by liquid phase oxidation,and the high-carbon alcohol was obtained by hydrolysis reaction of sodium hydroxide with the prepared boric acid ester.Then,infrared quantitative principle was used to analyse it.The optimum preparation conditions: The mole ratio of paraffin and boric acid was 1 to 4,the oxidation time was 6 h,the oxidation temperature was 170 ℃,the hydrolysis temperature was 80 ℃,the hydrolysis time was 1 h.The yield was about 12.7%.