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2008•Jilin Normal University JournalRequires access

Hydrothermal Synthesis and Characterization of a Vanadikum Phosphate (H_2NCH_2CH_2NH_2)_3 [V_9O_(12)(HPO_4)_6(PO_4)_2(H_2O)_2]·H_2O

Wei Liang

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Abstract

A novel inorganic-organic hybrid compound(H2NCH2CH2NH2)3[V9O12(HPO4)6(PO4)2(H2O)2]·H2O was synthesized under hydrothermal condition and it's structure was characterized by single-crystal X-ray diffraction,elemental analysis,TG analysis,IR spectrum.The title compound crystallize is a monoclinic crystal system,space P 21/n with crystal parameters a=14.324(3) ?,b=10.162(2) ?,c=18.367(4) ?,β=95.15°,V=2 673.5 ?3,Z=2.The compound not only has the laminated structure,but also has the column to support the nature and the pore characteristic.In addition,the compound has formed the formidable hydrogen bond function under the H2O and ethylene diamide.

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What this paper is about

A novel inorganic-organic hybrid compound(H2NCH2CH2NH2)3[V9O12(HPO4)6(PO4)2(H2O)2]·H2O was synthesized under hydrothermal condition and it's structure was characterized by single-crystal X-ray diffraction,elemental analysis,TG analysis,IR spectrum.The title compound crystallize is a monoclinic crystal system,space P 21/n with crystal parameters a=14.324(3) ?,b=10.162(2) ?,c=18.367(4) ?,β=95.15°,V=2 673.5 ?3,Z=2.The compound not only has the laminated structure,but also has the column to support the nature and the pore characteristic.In addition,the compound has formed the formidable hydrogen bond function under the H2O and ethylene diamide.

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Available abstract

A novel inorganic-organic hybrid compound(H2NCH2CH2NH2)3[V9O12(HPO4)6(PO4)2(H2O)2]·H2O was synthesized under hydrothermal condition and it's structure was characterized by single-crystal X-ray diffraction,elemental analysis,TG analysis,IR spectrum.The title compound crystallize is a monoclinic crystal system,space P 21/n with crystal parameters a=14.324(3) ?,b=10.162(2) ?,c=18.367(4) ?,β=95.15°,V=2 673.5 ?3,Z=2.The compound not only has the laminated structure,but also has the column to support the nature and the pore characteristic.In addition,the compound has formed the formidable hydrogen bond function under the H2O and ethylene diamide.

Key concepts: Monoclinic crystal system, Hydrothermal circulation, Crystallography, Hydrothermal synthesis, Crystal structure, Chemistry, Polyoxometalate, Ethylene

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Hydrothermal Synthesis and Characterization of a Vanadikum Phosphate (H_2NCH_2CH_2NH_2)_3 [V_9O_(12)(HPO_4)_6(PO_4)_2(H_2O)_2]·H_2O — Research Paper | ScholarLens